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各位,我们按EP药典检测辅料无水胶体二氧化硅含量的时候,对计算方法存在疑惑,请哪位大神能帮忙翻译一下,非常感激!
原文:To the residueobtained in the test for loss on ignition add 0.2 mL of sulphuric acid R andsufficient ethanol (96 per cent) R to moisten the residue completely. Add 6 mLof hydrofluoric acid R and evaporate to dryness on a hot-plate at 95-105℃, taking care to avoid loss fromsputtering. Wash down the sides of thedishwith6mL of hydrofluoric acid R andevaporate to dryness. Ignite at 900±50℃, allow to cool in a desiccatorand weigh.
The differencebetween the mass of the final residue and the mass of the residue obtained inthe test for loss on ignition gives the amount of SiO2 in thequantity of the substance to be examined used.
我们的理解是炽灼失重项下残渣与含量项下残渣的差值,比上供试品的称样量,即为SiO2的含量。
供应商的理解是含量=(炽灼失重项下残渣-含量项下残渣)/炽灼失重项下残渣
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